SIST ISO 5667-10:2021
(Main)Water quality - Sampling - Part 10: Guidance on sampling of waste waters
Water quality - Sampling - Part 10: Guidance on sampling of waste waters
This document contains details on the sampling of domestic and industrial waste water, i.e. the design of sampling programmes and techniques for the collection of samples. It covers waste water in all its forms, i.e. industrial waste water, radioactive waste water, cooling water, raw and treated domestic waste water.
It deals with various sampling techniques used and the rules to be applied so as to ensure the samples are representative.
Sampling of accidental spillages is not included, although the methods described in certain cases may also be applicable to spillages.
Qualité de l'eau - Échantillonnage - Partie 10: Guide pour l'échantillonnage des eaux résiduaires
Kakovost vode - Vzorčenje - 10. del: Navodilo za vzorčenje odpadne vode
General Information
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Standards Content (Sample)
SLOVENSKI STANDARD
01-januar-2021
Nadomešča:
SIST ISO 5667-10:1996
Kakovost vode - Vzorčenje - 10. del: Navodilo za vzorčenje odpadne vode
Water quality - Sampling - Part 10: Guidance on sampling of waste waters
Qualité de l'eau - Échantillonnage - Partie 10: Guide pour l'échantillonnage des eaux
résiduaires
Ta slovenski standard je istoveten z: ISO 5667-10:2020
ICS:
13.060.30 Odpadna voda Sewage water
13.060.45 Preiskava vode na splošno Examination of water in
general
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
INTERNATIONAL ISO
STANDARD 5667-10
Second edition
2020-11
Water quality — Sampling —
Part 10:
Guidance on sampling of waste water
Qualité de l'eau — Échantillonnage —
Partie 10: Lignes directrices pour l'échantillonnage des eaux
résiduaires
Reference number
©
ISO 2020
© ISO 2020
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting
on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address
below or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii © ISO 2020 – All rights reserved
Contents Page
Foreword .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 General aspects . 3
4.1 Design of sampling programme . 3
4.2 Sampling point selection - Representativeness . 3
4.3 Frequency and time of sampling . 4
4.3.1 Number of samples . 4
4.3.2 Sampling time for effluent stream . 4
5 Sampling at specific locations. 5
5.1 Sampling from sewers, channels and manholes . 6
5.2 Sampling from waste water treatments plants . 6
5.3 Sampling from industrial sites . 7
5.4 Sampling from cooling systems . 7
6 Main types of waste water sampling . 8
6.1 Spot sampling . 8
6.2 Composite sampling . 8
7 Waste water sampling . 9
7.1 General aspects . 9
7.1.1 Preparation of the sampling campaign . 9
7.1.2 Arrival on site . 9
7.2 Composite sampling for waste water quality monitoring .10
7.2.1 General.10
7.2.2 Automatic composite sampling .10
7.2.3 Manual composite sampling .13
7.2.4 Manual sample reconstitution .13
7.3 Spot sampling in an effluent stream .14
7.3.1 General.14
7.3.2 Direct sampling .15
7.3.3 Indirect sampling .15
7.3.4 Automatic, remote start or event-triggered sampling.16
7.4 Spot sampling of tanks — planned discharges .16
8 Sampling equipment .17
8.1 General .17
8.2 Automatic sampler .17
8.3 Manual sampling equipment .18
8.3.1 General.18
8.3.2 Ballasted sample collector .18
8.3.3 Bucket, vertical water sampler .18
8.4 Tank sampling equipment .19
8.4.1 Mixing .19
8.4.2 Sampling equipment . . .19
9 Homogenization, preservation, transport and storage of samples .19
9.1 Homogenization of collected volume .19
9.2 Distribution of collected volume into laboratory bottles .20
9.3 Preservation and packaging of samples .21
9.4 Transportation and reception .21
9.4.1 General.21
9.4.2 Time .21
9.4.3 Temperature .21
9.5 Security and traceability of samples during storage and delivery .22
9.5.1 Routine samples .22
9.5.2 Samples which might be used for legal purposes .22
10 Quality assurance .22
10.1 Avoidance of contamination .22
10.2 Sample identification and records .23
10.3 Assurance and quality control .23
11 Reports.23
11.1 Analytical reports .23
11.2 Sampling protocols .24
12 Safety precautions .24
12.1 General .24
12.2 Personnel safety .25
12.3 Equipment safety .25
Annex A (informative) Examples of sampling from tanks .27
Annex B (informative) Advantages and disadvantages of main types of waste water sampling .30
Annex C (informative) Example of cleaning protocol — Sampling equipment .32
Annex D (informative) Example of field form — Waste water sampling .34
Annex E (informative) Choice of compatible materials for automatic samplers .36
Annex F (informative) Comparison of types of pumping: peristaltic pump (PP) and vacuum
pump (VAP) .
...
INTERNATIONAL ISO
STANDARD 5667-10
Second edition
2020-11
Water quality — Sampling —
Part 10:
Guidance on sampling of waste water
Qualité de l'eau — Échantillonnage —
Partie 10: Lignes directrices pour l'échantillonnage des eaux
résiduaires
Reference number
©
ISO 2020
© ISO 2020
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting
on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address
below or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii © ISO 2020 – All rights reserved
Contents Page
Foreword .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 General aspects . 3
4.1 Design of sampling programme . 3
4.2 Sampling point selection - Representativeness . 3
4.3 Frequency and time of sampling . 4
4.3.1 Number of samples . 4
4.3.2 Sampling time for effluent stream . 4
5 Sampling at specific locations. 5
5.1 Sampling from sewers, channels and manholes . 6
5.2 Sampling from waste water treatments plants . 6
5.3 Sampling from industrial sites . 7
5.4 Sampling from cooling systems . 7
6 Main types of waste water sampling . 8
6.1 Spot sampling . 8
6.2 Composite sampling . 8
7 Waste water sampling . 9
7.1 General aspects . 9
7.1.1 Preparation of the sampling campaign . 9
7.1.2 Arrival on site . 9
7.2 Composite sampling for waste water quality monitoring .10
7.2.1 General.10
7.2.2 Automatic composite sampling .10
7.2.3 Manual composite sampling .13
7.2.4 Manual sample reconstitution .13
7.3 Spot sampling in an effluent stream .14
7.3.1 General.14
7.3.2 Direct sampling .15
7.3.3 Indirect sampling .15
7.3.4 Automatic, remote start or event-triggered sampling.16
7.4 Spot sampling of tanks — planned discharges .16
8 Sampling equipment .17
8.1 General .17
8.2 Automatic sampler .17
8.3 Manual sampling equipment .18
8.3.1 General.18
8.3.2 Ballasted sample collector .18
8.3.3 Bucket, vertical water sampler .18
8.4 Tank sampling equipment .19
8.4.1 Mixing .19
8.4.2 Sampling equipment . . .19
9 Homogenization, preservation, transport and storage of samples .19
9.1 Homogenization of collected volume .19
9.2 Distribution of collected volume into laboratory bottles .20
9.3 Preservation and packaging of samples .21
9.4 Transportation and reception .21
9.4.1 General.21
9.4.2 Time .21
9.4.3 Temperature .21
9.5 Security and traceability of samples during storage and delivery .22
9.5.1 Routine samples .22
9.5.2 Samples which might be used for legal purposes .22
10 Quality assurance .22
10.1 Avoidance of contamination .22
10.2 Sample identification and records .23
10.3 Assurance and quality control .23
11 Reports.23
11.1 Analytical reports .23
11.2 Sampling protocols .24
12 Safety precautions .24
12.1 General .24
12.2 Personnel safety .25
12.3 Equipment safety .25
Annex A (informative) Examples of sampling from tanks .27
Annex B (informative) Advantages and disadvantages of main types of waste water sampling .30
Annex C (informative) Example of cleaning protocol — Sampling equipment .32
Annex D (informative) Example of field form — Waste water sampling .34
Annex E (informative) Choice of compatible materials for automatic samplers .36
Annex F (informative) Comparison of types of pumping: peristaltic pump (PP) and vacuum
pump (VAP) .38
Annex G (informative) Type of distribution of collected volume into laboratory bottle .40
Annex H (informative) Quality control of sampling equipment .42
Annex I (informative) Bias and repeatability .44
Bibliography .45
iv © ISO 2020 – All rights reserved
Foreword
ISO (the Inte
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