General Information

Abstract

This European Standard specifies a calculation procedure for the determination of Iodine value ("CIV" - "calculated iodine value"), of fatty acid methyl esters (FAME) to be used either as automotive or heating fuel for diesel engines as specified in EN 14214 [2] or as an extender for automotive fuel for diesel engines as specified in EN 590 [4].
This procedure has originally been described in Annex B of EN 14214:2008 [2]. The calculation procedure is now specified for methyl esters between C14 and C24. The calculation procedure uses as data entry the results from the gas chromatography determination (GC) according to EN 14103 of individual fatty acid methyl esters and is based on AOCS recommended practice Cd 1c – 85 for the determination of the iodine value of edible oil from its fatty acid composition. It is important to recognise that the latest version of EN 14103 is to be used for the determination of individual FAME components.
NOTE 1   Experience from the field and from several precision evaluation campaigns in Germany and elsewhere indicates that the results of the determination of iodine value by calculation specified here are very close to results obtained by titration with Wijs solvent according to EN 14111. Observed small differences were always found to be smaller than the reproducibility published in the actual EN 14111.
For informative purposes only, but not for cases of dispute, EN 14331 [5] may also be used to extract the FAME contents from FAME containing diesel fuels (like B5, B7, B30, etc.) and to use the contents of the individual FAME components from this method as data entry for the calculation specified in this European Standard.
In principle, other fatty acid alkyl esters can also be analysed. However, neither the close correlation to the titration method EN 14111 has been verified nor is any precision information available for such an extension of application range.
NOTE 2   For the purposes of this European Standard, the term "% (m/m)" is used to represent the mass fraction, µ, of a material.

Status
Withdrawn
Publication Date
04-Sep-2012
Withdrawal Date
22-Sep-2026
Current Stage
9960 - Withdrawal effective - Withdrawal
Start Date
22-May-2024
Completion Date
23-Sep-2026

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18-Jan-2023
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28-Jan-2026
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Frequently Asked Questions

EN 16300:2012 is a standard published by the European Committee for Standardization (CEN). Its full title is "Automotive fuels - Determination of iodine value in fatty acid methyl esters (FAME) - Calculation method from gas chromatographic data". This standard covers: This European Standard specifies a calculation procedure for the determination of Iodine value ("CIV" - "calculated iodine value"), of fatty acid methyl esters (FAME) to be used either as automotive or heating fuel for diesel engines as specified in EN 14214 [2] or as an extender for automotive fuel for diesel engines as specified in EN 590 [4]. This procedure has originally been described in Annex B of EN 14214:2008 [2]. The calculation procedure is now specified for methyl esters between C14 and C24. The calculation procedure uses as data entry the results from the gas chromatography determination (GC) according to EN 14103 of individual fatty acid methyl esters and is based on AOCS recommended practice Cd 1c – 85 for the determination of the iodine value of edible oil from its fatty acid composition. It is important to recognise that the latest version of EN 14103 is to be used for the determination of individual FAME components. NOTE 1 Experience from the field and from several precision evaluation campaigns in Germany and elsewhere indicates that the results of the determination of iodine value by calculation specified here are very close to results obtained by titration with Wijs solvent according to EN 14111. Observed small differences were always found to be smaller than the reproducibility published in the actual EN 14111. For informative purposes only, but not for cases of dispute, EN 14331 [5] may also be used to extract the FAME contents from FAME containing diesel fuels (like B5, B7, B30, etc.) and to use the contents of the individual FAME components from this method as data entry for the calculation specified in this European Standard. In principle, other fatty acid alkyl esters can also be analysed. However, neither the close correlation to the titration method EN 14111 has been verified nor is any precision information available for such an extension of application range. NOTE 2 For the purposes of this European Standard, the term "% (m/m)" is used to represent the mass fraction, µ, of a material.

This European Standard specifies a calculation procedure for the determination of Iodine value ("CIV" - "calculated iodine value"), of fatty acid methyl esters (FAME) to be used either as automotive or heating fuel for diesel engines as specified in EN 14214 [2] or as an extender for automotive fuel for diesel engines as specified in EN 590 [4]. This procedure has originally been described in Annex B of EN 14214:2008 [2]. The calculation procedure is now specified for methyl esters between C14 and C24. The calculation procedure uses as data entry the results from the gas chromatography determination (GC) according to EN 14103 of individual fatty acid methyl esters and is based on AOCS recommended practice Cd 1c – 85 for the determination of the iodine value of edible oil from its fatty acid composition. It is important to recognise that the latest version of EN 14103 is to be used for the determination of individual FAME components. NOTE 1 Experience from the field and from several precision evaluation campaigns in Germany and elsewhere indicates that the results of the determination of iodine value by calculation specified here are very close to results obtained by titration with Wijs solvent according to EN 14111. Observed small differences were always found to be smaller than the reproducibility published in the actual EN 14111. For informative purposes only, but not for cases of dispute, EN 14331 [5] may also be used to extract the FAME contents from FAME containing diesel fuels (like B5, B7, B30, etc.) and to use the contents of the individual FAME components from this method as data entry for the calculation specified in this European Standard. In principle, other fatty acid alkyl esters can also be analysed. However, neither the close correlation to the titration method EN 14111 has been verified nor is any precision information available for such an extension of application range. NOTE 2 For the purposes of this European Standard, the term "% (m/m)" is used to represent the mass fraction, µ, of a material.

EN 16300:2012 is classified under the following ICS (International Classification for Standards) categories: 75.160.20 - Liquid fuels; 75.160.40 - Biofuels. The ICS classification helps identify the subject area and facilitates finding related standards.

EN 16300:2012 has the following relationships with other standards: It is inter standard links to EN 16300:2024, EN 14103:2020, EN ISO 12354-1:2017, EN 14214:2012+A2:2019, EN 14214:2012+A1:2014, EN ISO 10848-1:2006, EN ISO 717-1:2013, EN 14214:2012. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

EN 16300:2012 is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.

Standards Content (Sample)


2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Kraftstoffe für Kraftfahrzeuge - Bestimmung der Iodzahl - Berechnung aus gaschromatografischen DatenCarburants pour automobiles - Détermination de la valeur iodique - Méthode de calculation par dates de chromatographie en phase gazeuseAutomotive fuels - Determination of iodine value - Calculation method from gas chromatographic data75.160.20Liquid fuelsICS:Ta slovenski standard je istoveten z:EN 16300:2012SIST EN 16300:2012en,de01-november-2012SIST EN 16300:2012SLOVENSKI
STANDARD
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 16300
September 2012 ICS 75.160.20 English Version
Automotive fuels - Determination of iodine value in fatty acid methyl esters (FAME) - Calculation method from gas chromatographic data
Carburants pour automobiles - Détermination de l'indice d'iode dans les esters méthyliques d'acides gras - Méthode de calcul à partir des données obtenues par chromatographie en phase gazeuse
Kraftstoffe für Kraftfahrzeuge - Bestimmung der Iodzahl in Fettsäure-Methylester (FAME) - Berechnung aus gaschromatographischen Daten This European Standard was approved by CEN on 27 July 2012.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2012 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 16300:2012: ESIST EN 16300:2012

This procedure has originally been described in Annex B of EN 14214:2008 [2]. The calculation procedure is now specified for methyl esters between C14 and C24. The calculation procedure uses as data entry the results from the gas chromatography determination (GC) according to EN 14103 of individual fatty acid methyl esters and is based on AOCS recommended practice Cd 1c – 85 for the determination of the iodine value of edible oil from its fatty acid composition. It is important to recognise that the latest version of EN 14103 is to be used for the determin
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